Wait a second!
More handpicked essays just for you.
More handpicked essays just for you.
State the application of IR spectroscopy
Conclusion steam distillation
Don’t take our word for it - see why 10 million students trust us with their essay needs.
Recommended: State the application of IR spectroscopy
Steam Distillation
Purpose: To use steam distillation to purify heat sensitive, natural products, like essential oils.
Procedure
Please refer to:
Williamson, Macroscale &Microscale Organic Experiments 4th Ed., pgs.98-109
Results
Table 1.1: Steam distillation
Drop # (every third drop) Temperature (ºC) Addition of 0.5 mL water
1 100.3 Water added
2 100.5
3 100.5 Water added
4 100.6 Water added
5 100.6
6 100.6 Water added
7 100.6
8 100.6 Water added
9 100.3
10 100.6
Observations: The residue was cloudy during distillation. This indicated that it was wet. The water was added when the solution appeared to be getting low in volume.
Table 1.2: Recovery of organic material
Object being weighed Weight in grams
Weight of empty, clean test tube 6.446 g
Weight of clean test tube with spearmint oil 6.635 g
Weight of spearmint oil 0.189 g
Table 1.3: IR Spectroscopy
Frequency Corresponding Functional Group
3083.81 C-H
2923.91 C-H
1674.33 C=O
Conclusion
In this experiment, the process of steam distillation was used to purify a natural product, (the essential oil of spearmint). This phenomenon works because when two immiscible liquids are distilled, the boiling point of the mixture is below the boiling point of the both pure compounds. Since water has a significantly lower boiling point than spearmint, a much greater proportion of water molecules was vaporizing at any time during the distillation. Even though the components of spearmint oil have low vapor pressure, they are volatile enough to vaporize to some extent and a small amount will lifted off with the water molecules. This boiling will occur when the independent internal vapor pressures are equal to 760 torr, which is the external vapor pressure. It is noted that steam distillation, unlike regular distillation, it does not follow Raoult’s Law.
After steam distillation was completed, the essential oil was recovered and a thin layer chromatography was conducted. When this TLC was conducted, there was one spot of pure essential oil and one of the distilled and recovered essential oil. The results indicated that the distilled, recovered oil was pure because it came out as a single spot, level with that of the pure oil. The infrared spectroscopy was performed next. IR spectroscopy is used to identify the functional by stretching and bonding frequencies of bonds. The peaks correspond to the functional groups.
Introduction In this experiment, steam distillation was used to isolate eugenol oil from cloves. The goal of this experiment was to test and analyze the purity level of the eugenol oil that was isolated by applying a TLC test as well as H-NMR spectra. At the end of this experiment, eugenol oil was isolated, but some errors that occurred during the experiment resulted in impurities in the final isolated oil.
Once the mixture had been completely dissolved, the solution was transferred to a separatory funnel. The solution was then extracted twice using 5.0 mL of 1 M
A condenser and heat reflux was used to prevent reagents from escaping. Then the solid product was vacuum filtered. The product was recrystallized to purify it and the unknown
In the first part of the experiment, The mixture was combined with saturated sodium chloride, and the aqueous layer, containing alcohol, some acid, and water, was discarded. The organic layer was then dried with granular anhydrous sodium sulfate; this drying agent is used to absorb any water in a solution and should thus, result in a colorless solution. The final product was collected; it was mostly clear, though it has a pale yellow tint. Data Table 2 shows the results and calculations that were gathered after the completion of this experiment. No errors had occurred during the course of the experiment, which is testified by the fairly, high yield of Data Table 3 indicates the observations from these tests.
The objective of this experiment was to perform extraction. This is a separation and purification technique, based on different solubility of compounds in immiscible solvent mixtures. Extraction is conducted by shaking the solution with the solvent, until two layers are formed. One layer can then be separated from the other. If the separation does not happen in one try, multiple attempts may be needed.
Afterwards, we conducted crystallization to evaporate the liquid in an attempt to detect the presence of a salt. Before stating which of the potential
Performing this experiment, we used the technique called Acid-Base extraction to isolate Eugenol, which is one of the main ingredients of clove oil. Acid-Base extraction is the most efficient method for isolating organic component; it is efficient because it purifies the acid and base mixture based on their chemical identities. We have seen throughout this experiment that acid and base play an important role, when it comes to solubility in water. Our basic knowledge of acid and base is acid is a proton donor and base is a proton acceptor. This ideology helps us to understand why organic compounds are not soluble in water. When compounds tend to be insoluble, we have to use acid and base reaction, to change its solubility. The changes that occurred
== Refer to, Chemistry Lab #1 – What’s the substance? However, I changed some of procedures during my experiment, here is the changes I made in this experiment: * I only used the toothpick to place a small amount of each sample on a separate piece of paper, instead of the spatula.
What is aromatherapy? In an article titled “Phytotherapy Research” by Amr Edris, he describes aromatherapy as, “The use of essential oils and their volatile constituents are widely to prevent and treat human disease.” Aromatherapy is said to be an alternate form of medicine that uses essential oils, which are made up of volatile plant materials. With these essential oils it is said that they help to alter a person’s mood, health, mind, and cognitive function. It is also said that aromatherapy could substitute as treatment or prevention for certain diseases. There are many different types of oils used for aromatherapy in different ways for different outcomes. Such methods include the topical application, aerial diffusion, and direct inhalation. Topical application is any direct contact with the oil, used such as placing the oil in a bath or directly on to the skin. Aerial diffusion is where the oil is placed on the carpet around you or even on to a pillow or bed. Direct inhalation is a method where the oil is placed on the hands and rubbed together then while cupping your hands under your face to inhale the oils, this has a very powerful effect when used. Some uses of aromatherapy are for used as anti-depressants, relive stress, help with relaxation, insomnia, acne, itching and many more. To cure anxiety lavender, chamomile, rose, vanilla, and cardamom oils are all used for this. Lemon, jasmine, rosemary, sandalwood, and peppermint oils are all used to help with depression. When dealing with fatigue it is said that basil, cedarwood, clove, and eucalyptus all help. Headaches can be cured with lemon grass, thyme, ginger, and cinnamon oils. Caraway, chamomile, lavender, and rosemary oils are all used to help with menstrual cramps. The...
As the pressure drop increases in the column, it is observed that the degree of foaming becomes more violent and more spread out. When the pressure drop is relatively high, it means that the pressure exerted by the vapour is insufficient to hold up the liquid in the tray, causing the gas bubbles to appear on top of the sieve trays. To add on, the higher the pressure drop, the higher the velocity of the vapour passing up the column. As a result, more vapour will penetrate the liquid and more bubbles formation is observed. Due to more bubbles formation, the degree of foaming are more agitated, rapid and spread out.
The first group of chemical compounds to be discussed are terpenes. Terpenes are a very comprehensive group of metabolites which are known to contain essential oils that produces well-known scents in herbs belonging to the Lamiaceae plant family (Scott 2008). These scented compounds are usually found in the trichomes of basil, rosemary, lavender, etc. (Scott 2008). Electron micrograph images of these trichomes can be seen below. According to Keeling & Boltmann (2006), there are about 30 000 known types of terpenes which originated from structures created from terpene synthases. These terpene synthases can be broken up into three groups, monoterpene synthases, sesquiterpene synthases, and diterpene synthases (Keeling &...
If the solid dissolved in the solvent at room temperature, then it was too soluble and that solvent could be eliminated. The acetanilide is completely dissolved in ethanol and dichloromethane, therefore eliminating them from being the suitable solvent. If the solid did not dissolve at room temperature then it was placed in the sand bath and left to boil. If the solid dissolved, it was placed in the ice bath and if crystals were observed coming out of the solution then the suitable solvent was found. The suitable solvent was water as the crystals came out once placed in the ice bath.
Eugenol was extracted from cloves through the process called steam distillation. A total of 50ml of distillate were collected with temperature monitoring for every 5.0ml of collected liquid. The distillation curve showed that the temperature of volatilization of eugenol is from 98°C to 99°C which is way below its boiling point at 2540C. Chemically active extraction was conducted in order to remove impurities particularly eugenol acetate and caryophyllene. This involves the addition of several solvents particularly hexane, NaOH, HCl, then hexane again in succession.
Essential oils were used by the ancient Egyptians’ to produce perfumes. They spent hundreds’ of years’ trying to perfect beautiful smel...
Besides the use of essential oils in fragrances, there are approximately 3000 chemicals that are used in making of fragrance. It is used in many body care products and as well as perfumes, colons, and deodorants. As the studies have shown, such chemicals can trigger many different feelings hunger, nostalgia, happiness, or disgust. It is also used in many home products such as candles, cleaning products, laundry detergents, fabric care, and air fresheners. Fragrances are made with essential oils, which consists of extract of a plant. However, about 95 percent of the ing...