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Introduction about laboratory techniques
General laboratory techniques 1
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Chemistry: Acid-Base Titration
Purpose:
The objective of this experiment were: a) to review the concept of simple acid-base reactions; b) to review the stoichiometric calculations involved in chemical reactions; c) to review the basic lab procedure of a titration and introduce the student to the concept of a primary standard and the process of standardization; d) to review the calculations involving chemical solutions; e) to help the student improve his/her lab technique.
Theory:
Titration was used to study acid-base neutralization reaction quantitatively. In acid-base titration experiment, a solution of accurately KHP concentration was added gradually to another solution of NaOH concentration until the chemical reaction between the two solutions were completed. The equivalence point was the point at which the acid was completely reacted with or neutralized by the base. The point was signaled by a changing of color of an indicator that had been added to the acid solution. Indicator was substance that had distinctly different colors in acidic and basic media. Phenolphthalein was a common indicator which was colorless in acidic and neutral solutions, but reddish pink was result in basic solutions. Strong acid (contained H+ ion) and strong base ( contained OH ) were 100% ionized in water and they were all strong electrolytes. Procedure:
Part A. Investigating solid NaOH for use as a possible primary standard First o...
taken into account. It is also best to make sure you are working in a
== Volume of NaOH used is recorded below: Trial (cm3) 1st time (cm3) Initial burette reading 3.55 18.4 Final burette reading 22.8 36 Titre 19.25 17.6 pH Chloroethanoic acid 3.0 Dichloroethanoic acid 2.2 Ethanoic acid 4.6 pH of chloroethanoic acid and dichloroethanoic acid is given by the teacher. Calculation: = ==
in 50 ml of water, and finally titrated the base three different times, we could then
The equation shows how 1 mol of Na2CO3 reacts with 1 mol of H2SO4, so
Acid-Base Titration I. Abstract The purpose of the laboratory experiment was to determine equivalence. points, pKa, and pKb points for a strong acid, HCl, titrated with a. strong base, NaOH using a drop by drop approach in order to determine. completely accurate data. The data for this laboratory experiment is as follows.
Some improvements to the experiment might be using Na Acetate or Na Citrate as buffers instead of KHPO4. The pH ranges are 4.5-5.5 and 4.7-5.5, respectively. This range falls closer to the ideal pH of 5, then KHPO4 (pH
The same procedure was done using 10ml of CV and 20ml of sodium hydroxide, both separately diluted to 50ml and added in a large beaker. The absorbance was recorded. In the last trial, 10ml of CV, 10ml of NaOH were diluted to 50ml. Before adding the two mixtures, 1ml of soap was added to the NaOH solution and then poured into a large beaker, along with the CV. Absorbance was recorded and the materials
The simplest experiment for this type of situation would be to use red and blue litmus paper to distinguish between acids, bases and salts. Hydrochloric acid (HCl) makes blue litmus paper change color going from blue to red, making it an acid. Sodium hydroxide (NaOH) makes red litmus paper change color going from red to blue, making it a base. Sodium chloride solution (NaCl) is neutral, since it would only soak blue and red litmus paper, considering that it is a by product of when an acid and a base mix together, neutralizing each other.
Acid-Base balance is the state of equilibrium between proton donors and proton acceptors in the buffering system of the blood that is maintained at approximately pH 7.35 to 7.45 under normal conditions in arterial blood. It is important to regulate chemical balance or homeostasis of body fluids. Acidity or alkalinity has to be regulated. An acid is a substance that lets out hydrogen ions in solution. Strong acid like hydrochloric acid release all or nearly all their hydrogen ions and weak acids like carbonic acid release some hydrogen ions.
Rinse a 25mL buret with three 5mL portions of standard permanganate solution. Fill the buret with the standard permanganate solution and record initial and final readings.
Titration is a technological process in which a solution, known as a titrant, is slowly and carefully added from a burrette into a fixed volume of another solution (known as the sample). In an acid-base titration an acid neutralizes a base or vice versa. This process is maintained untill the reaction between the titrant and the sample (acid and the base) is judged to be complete. The reaction is judged to be complete when the endpoint is reached. An endpoint in a titration analysis is referred to as the point at which no more titrant is added due to an observable colour change of an indicator. Indicators can be used to find an endpoint because they change colour when the pH of a solution changes and an endpoint in a titration is an empirical approximation of the equivalence point, which is the point of major pH change in the titration sample due to the fact that equal chemical amounts of reactants have been combined at that point. All indicators have a pH range, which is the range of pH values at which the colour of the indicator changes. Thus
1. The key factor I plan to investigate and what I will do to make my
borate) and 1.0 g. of sodium hydroxide in 20 mL of warm water. It may
In this experiment three different equations were used and they are the Stoichiometry of Titration Reaction, Converting mL to L, and Calculating the Molarity of NaOH and HCl (Lab Guide pg. 142 and 143).
the left so that the concentration of H is more than Me and so the