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Explain titration essay
Titration practical writeup
Pratical for titration
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To undertake titration and colorimetry to determine the concentration of solutions
By carrying out titrations and colorimetry, the aim of this investigations was to use these methods such that the concentrations of different solutions used can be identified, and to help find the concentration of the unknown solution that were given. Using Titration and colorimetry the concentrations of different solutions in general can be determined and this helps to identify solutions with unknown concentrations. In this assignment I was asked to carry out two different scientific techniques and find the concentration of different solutions.
Titration of sodium carbonate and sodium hydroxide
I was asked to find the concentration of a solution of sodium
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The equipment I had to calibrate was a pipette, top pan balance and a pH meter. Calibration is a marking a scale on a measuring instrument. This involves establishing the relationship between indications of a measuring instrument and standard or reference quantity values, which must be applied. Calibration is important when conducting an experiment. For example, broken or wrongly calibrated pH meters can give incorrect results, making the results useless. In a research laboratory this could lead to wrong conclusions, wasted time and wasted …show more content…
Its concentration is usually given in mol dm-3. A standard solution is created using a powdered form of the substance and dissolving it in distilled water to make a solution where you know the concentration. When making up a standard solution it is important that the correct mass of substance is accurately measured. It is also important that all of it is transferred to the volumetric flask used to make up the solution. The following procedure will make sure that this happens. Using these solutions will contain accurate concentrations of a chemical component, they will increase confidence regarding the determination of substances with unknown concentrations.
Colorimeter to determine the concentration of two unknown solutions
A colorimeter is a device used to test the concentration of a solution by measuring its absorbance of a specific wavelength of light. It can be used for coloured solutions of different concentrations. Before it can be used I had to calibrate the colorimeter. To do this I had to calibrate a colorimeter a cuvette filled with distilled water is placed into the colorimeter, the colorimeter in theory should then give a reading of the absorbance level being 0, this is because the water used in the calibration process is distilled and therefore should give a reading of 0, if not then it shows the equipment being used the experiment is either faulty or inaccurate. As all the light will pass
Record the volume of the sodium thiosulfate solution used in the titration, and repeat the procedure in a duplicate titration.
Once the mixture had been completely dissolved, the solution was transferred to a separatory funnel. The solution was then extracted twice using 5.0 mL of 1 M
We were assigned a group and instructed to measure the amount of different ions in that particular fertilizer sample by counting to preform tests. We used the formula SO4 + Agent —> Percipitat + others. Our job was to add 0.25 g of a fertilizer sample to 100 mL of water to dissolve, then add the agent Pb(NO2)3 to the water also, then filter and dry the water, and distinguish the mass. The was accomplished by using the % formula Mass SO4 = Mass Pb(NO3)2 x MW Pb(NO3)2/ MWPb(NO3)2 to gain the percentage, the the formula Mass SO4/MW SO4 =
We were then to make a base solution of 0.7 M NaOH. In order to standardize
Using a concentration of.1 NaOH. We had the largest NaOH volume before the largest pH increase at 6.38ml. For the largest NaOH volume after the largest pH increase we used 6.73ml of base. The volume of NaOH used at the equivalence point, pH 7, was 6.575ml. The moles of NaOH used at this point were.0006575mols.
By doing this experiment, I can know the physical and chemical properties of these samples. After I get my results about the physical and chemical properties of these samples, I can compare my results with the information given by the past student and identify the 5 unknown samples, finding out which sample is which substance. Hypothesis = ==
...s strength in the experiment rather than a limitation which future studies should also monitor.
We were not given any instructions either to shake or not to shake the test tubes with the coloured solutions before inserting them in the spectrophotometer to read the absorbance. By shaking each test tube a certain number of times before putting it in the spectrophotometer could have improved the accuracy of the of absorbance of the solutions.
The same procedure was done using 10ml of CV and 20ml of sodium hydroxide, both separately diluted to 50ml and added in a large beaker. The absorbance was recorded. In the last trial, 10ml of CV, 10ml of NaOH were diluted to 50ml. Before adding the two mixtures, 1ml of soap was added to the NaOH solution and then poured into a large beaker, along with the CV. Absorbance was recorded and the materials
= = = Electronic Balance (accurate to 2 decimal places) Goggles Spatula Distilled Water ( 250cm3) Anhydrous Sodium Carbonate (2.65g) Beaker - 250cm3 Stirring Rod Petri Dish Pipette Volumetric flask Requirements for the titration experiment: - =
Determining the Concentration Of Limewater Solution Aim: The aim of this experiment is it to find out the concentration of Limewater by performing a titration with hydrochloric acid which has concentration exactly 2.00M.. What is required for me is that I have to design my own experiment and chose the right and appropriate apparatus and equipment. I will be provided with 250cm3 of limewater, which has been made to which contains approximately 1g/dm3 of calcium Hydroxide. This hypothesis from www.studentcentral.co.uk We were also give Hydrochloric acid (HCl) with a concentration of 2.00 mol/dm3 normal laboratory apparatus was also given and so was an indicator.
The purpose of this experiment is to use our knowledge from previous experiments to determine the exact concentration of a 0.1M sodium hydroxide solution by titration (Lab Guide pg.141).
2. Photometer; after the chosen range of wavelength of light passes through the solution of a sample in cuvette, the photometer detects the amount of photons that is absorbed and then sends a
If someone needed a test that was more accurate and detailed to analysis how accurately they can see perceive colors, they would need to take a quantitative color blind test. The most popular test to use is the Farnsworth-Munsell 100 hue test. The test consists of four trays containing many small disks of varying hues. Each tray has a color reference disk at one end. The person being tested must arrange the other disks within the tray to create a continuum of gradually changing hue.
A refractometer is an optical device that is used to measure the optical density or refractive index of a substance. Refractive index is a dimensionless number that describes how light, or any other radiation is bent as it moves through a medium. It is the ratio of light’s velocity in a vacuum (n=1) to its velocity in the sample. The greater the increase in optical density or refractive index, the greater the speed of light is reduced in a solid, gas or solution. A refractometer measures the refractive index of liquids, gases and translucent solids like gemstones. There are four main types of refractometers: traditional handheld refractometers, digital handheld refractometers, laboratory or Abbe refractometers, and inline process refractometers, (Wikipedia - Refractometers). Scientists often use refractometers to measure the refractive index when studying the physical properties of different solids and liquids. Bench and handheld refractometers are usually used for more practical purposes, for example to measure the concentration of a dissolved substance.