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Density measurement in lab technique
Density measurement in lab technique
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The Empirical Formula of Magnesium Oxide
Aim.
To find out the empirical formulae for magnesium-oxide
Introduction.
The empirical formula of a compound tells us the types of atoms present in a compound as well as the simplest whole-number ratio of the different types of atoms. The empirical formula does not tell us the actual number of atoms in the molecule.
The mass of Mg + the mass of O2=mass of MgxOx. Knowing the mass of magnesium used and the mass of magnesium oxide produced you can determine the mass of oxygen used. The ratio between number of moles of magnesium used and number of moles of oxygen used can be calculated and the empirical formula can be written on the basis of
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Gauze
4. Crucible and Lid
5. Tongs
6. Heatproof mat
7. Safety glasses
8. Magnesium
Diagram.
Method.
1. Place a clean, dry crucible (check for any cracks) with its cover on a clay triangle supported by a tripod. Adjust the flame of a Bunsen burner so that the crucible is just above the hot part of the flame. Heat the crucible strongly for five minutes. The bottom of the crucible should glow red during the heating.
2. Remove the crucible, using the crucible tongs, and place it on the ceramic pad to cool. After the crucible has cooled to room temperature (this will take about ten minutes), weigh it with its cover on an analytical balance to 0.001 g. Record the weight on the data sheet.
3. Weigh out 0.3g of magnesium and place it into the crucible. Weigh the magnesium, crucible and cover on an analytical balance. Record the weight to 0.001 g.
4. At frequent intervals, remove the burner and slightly lift the crucible lid using tongs, quickly replacing the lid so as to lose as little magnesium oxide 'smoke' as possible. Repeat the process patiently until the magnesium ceases to flare up, then remove the
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You should not be able to see any shiny metallic surfaces. Allow the crucible to cool then replace the lid and reweigh the whole. Record the mass.
5. Repeat this 5 times so that you will be able to gain an average result.
Fair Test.
To make this a fair test we weighed the empty crucible and lid before adding magnesium. This means that the different weights of the crucibles could be accounted for. This allowing any minor errors in the experiments result to be averaged out. To make this a lot more accurate we carried the test out 5 times.
Before each time we carried out the experiment we cleaned the crucible and lid thoroughly making sure that there was no excess foreign materials of any sort to tamper with the chemical reaction.
m= 10km2 x 1000m x 1000m = 107m2 107m2 x 15= 1.5 x 1.8m3 = 1.5 x 1011kg
The Gravimetric Stoichiometry lab was a two-week lab in which we tested one of the fundamental laws of chemistry: the Law of Conservation of Mass. The law states that in chemical reactions, when you start with a set amount of reactant, the product should theoretically have the same mass. This can be hard sometimes because in certain reactions, gases are released and it’s hard to measure the mass of a gas. Some common gases released in chemical reactions include hydrogen, carbon dioxide, oxygen and water vapor. One of the best methods for determining mass in chemistry is gravimetric analysis (Lab Handout).
Mass of O = Mass of crucible, cover, KClO3 and MnO2 after heating (Step # 11) - Mass of crucible, cover, KClO3 and MnO2 before heating (Step # 5)
Aim: The aim of this experiment was to determine the empirical formula of magnesium oxide.
Get together a clay triangle, ringstand, and a burner. Wash a crucible. Locate the crucible onto the ringstand. Warm the crucible on the scorching section of the flame from the burner for approximately five minutes. Chill the crucible at room temperature. Then, weigh it precisely. Grasp the crucible using tong because the use of hands will add oils and residues on to crucible. Place roughly 2 grams of copper sulfate inside the crucible. Then, measure the weight of the crucible along with its contents. Position the crucible onto the clay triangle. Next, heat up the crucible steadily at the beginning to avoid splattering. Once heated to the shade of red, place on the hot part of the bunsen burner flame for precisely five minutes, chill to room temperature, and find the mass of the crucible including its contents. Document the weight on the data sheet. Put the crucible on the ringstand. Pour a small about of distilled water into the crucible. Wait about five minutes to see reaction that is made. Find the mass of the crucible. Indicate the mass on data sheet.
find the rate I have to find the mass change in 1 hour, and I will
In this lab, I determined the amount of heat exchanged in four different chemical reactions only using two different compounds and water. The two compounds used were Magnesium Hydroxide and Citric Acid. Both compounds were in there solid states in powder form. Magnesium Hydroxide was mixed with water and the change in heat was measured using a thermometer. The next reaction combined citric acid and magnesium hydroxide in water. The change in heat was measured as well. For the third reaction citric acid was placed in water to measure the change in heat. In the last reaction, citric acid was combined with water. The heat exchanged was again measured. It is obvious we were studying the calorimetry of each reaction. We used a calorimeter
I am going to carry out an experiment to measure the change in mass of
Reaction 2: H = 50 x 4.18 x -10.3" H = -2152.7 This value is for 1.37g of calcium oxide, not 56.1g, which is its relative molecular mass. Therefore: H =
with a tong to see if the magnesium had started to burn and also to
of Copper Sulphate. To do this I plan to work out the amount of water
3 cm of magnesium ribbon generally has a mass of 0.04 g and yields 40 cm3 of hydrogen when reacted with excess acid. 50 cm3 of 1M hydrochloric in this experiment is in excess.
Measure the mass of the trolley and then measure the mass of the mass piece