In this experiment, NaOH and diethyl ether are used as solvents. NaOH and diethyl ether must be immiscible with one another. They each must selectively attract the desired component from the solution being extracted. They should be easily separable from the solute being used. NaOH is a polar solvent and dissolves benzoic acid that has a high polarity, while diethyl ether is a nonpolar solvent and dissolves naphthalene that has a low polarity. The density determines the solvent position in the separatory
Reaction Equation Summary In this experiment a Grignard reaction was carried out to give the desired reagents: benzyl magnesium chloride. This was achieved by reacting benzyl chloride with magnesium in ether. After the Grignard’s reagents were formed, it was reacted with benzaldehyde in ether to give 1,2-diphenylethanol. The main objective of this experiment was to synthesize 1,2-diphenylethanol via a Grignard reaction. The NMR proves that the right product was formed in this experiment. Introduction
using an organic solvent like diethyl ether and a polar solvent such as water. Diethyl ether is an appropriate solvent since it wil... ... middle of paper ... .... Conclusions and Future Experiments: How would you summarize your results and analysis? What questions remain unanswered? What questions were raised by your results and analysis? In summary, acid base extraction is a useful technique when attempting to transfer an organic compound from an organic solvent (ether) to an aqueous solvent after
mixture of fluorene, o-toluic acid, and 1, 4-dibromobenzene, the previously learned techniques of extraction and crystallization are needed to perform the experiment. First, 10.0 mL of diethyl ether would be added to the mixture in a centrifuge tube (1) and shaken until the mixture completely dissolved (2). Diethyl ether is the best solvent for dissolving the mixture, because though it is a polar molecule, its ethyl groups make it a nonpolar solvent. The compounds, fluorene and 1, 4-dibromobenzene, are
(0.470 mL, 0.6533 g, 5.40 mmol) were charged with stir bar and stirred at room temperature for 45 minutes. Diethyl ether (10 mL) was added to the reaction mixture and stirred. The mixture was gravity filtered into a beaker that was topped with a watchglass. The filtrate was transferred to a separatory funnel and the organic layer was extracted with deionized water (10 mL) and diethyl ether (15 mL). The organic layer was placed into an Erlenmeyer flask and the aqueous layer was placed into a beaker
Chloroform is an anesthetic that is inhaled, and was once a widely used one. However, nowadays it isn’t because of its toxic side effects. Chloroform is another name for the colorless, dense, liquid chemical compound trichloromethane. Chloroform is nearly 40 times as sweet as sugar and has a nice odor. It is inflammable and can be used for industrial purposes like R-22 (air-conditioning), a solvent, a fire extinguishing material, and as a chemical reagent for use in synthetic reactions. Its primary
The Discovery and Controversy over the First Use of Surgical Anesthesi Dennis Brindell Fradin wrote in ”We Have Conquered Pain”: The Discovery of Anesthesia, “We take it for granted that we can sleep through operations without feeling any pain. But until about 150 years ago, the operating room was a virtual torture chamber because surgeons had no way to prevent the pain caused by their healing knives.” Fradin is right. Since several analyses of archaic human bones have proven that people have
Hundreds of household products are being misused as inhalants. Some of these products include nail polish remover, hair spray, cleaning fluids, spray paint, and the propellant in aerosol whipped cream (“Inhalants“, 2010). Inhalants are breathable chemical vapors that users intentionally inhale because of the chemical’s mind-altering effects (National Institute on Drug Abuse [NIDA], 2010). The trend in inhalant abuse is growing among the young community throughout the country. Surveys have shown in
Identifying features and key components of unknown chemical mixtures are an essential part of chemistry. In many cases it is necessary to analyses and understand the chemical makeup of pharmaceuticals. Qualitative analysis is a method of testing a chemical mixture to determine its chemical makeup, such as its functional group. Identifying functional groups of an unknown compound are important, as it helps in understanding how a chemical acts under certain conditions, such as when changing physical
Eugenol (C10H12O2) is a well-known natural product occurring in many plants like cloves and nutmeg, with a satisfying scent and spicy taste. Eugenol is extracted from numerous aromatic plants and used in perfumeries for spicy, clove-like and oriental-type fragrances. “Alike all phenols, eugenol is an antiseptic; used as disinfectant in mouthwash. Due to its antiseptic and analgesic properties, it is used in dentistry; upon mixing with zinc oxide it forms cement for temporary fillings of the teeth
Oxidation of a Secondary Alcohol with Chromic Acid in Diethyl Ether to Produce a Ketone Compound Amber Breakspear 15202075 – 12th January 2016 Year 1 Full Report 1 – Organic Abstract An effective oxidation of the secondary alcohol with chromic acid to produce the corresponding ketone. In this report the synthesis of 4-methyl-2-pentanone from 4-methyl-2-pentanol via an adapted jones oxidation1, using diethyl ether as the solvent and concentrated sulphuric acid, is described. An
product RMgX which is known as Grignard reagent. The Grignard reagent formation always undergoes through dry anhydrous ether solvent due to its ability to act as Lewis base (donates pair of electrons) which is necessary to solvate and stabilize the RMgX Grignard reagent. In this experiment, the aryl halide bromobenzene was reacted with magnesium turnings in anhydrous diethyl ether solvent to form the Grignard reagent, phenylmagenisum bromide. It is very important and necessary that all reagent, solvent
layer of the separatory funnel. For extraction to be used as an effective method for separation, the components of a mixture that need to be recovered must not be soluble in the same solvent. Benzoic acid is not soluble in water, but is soluble in diethyl ether. In benzoic acid, the benzene ring is nonpolar
acetic acid only if acetic acid is cheap, and if unreacted acetic acid can be removed easily from the product mixture (Organic chemistry lab. Manual, p32). In this lab had to use acid- base extraction process. Since isopentyl acetate is soluble in diethyl ether, but acetic acid is soluble in both solvents. Therefore, a simple extraction procedure would remove only some of the acetic acid from isopentyl acetate, but it would not completely separate the two compounds. An acid-base extraction improves on
This causes the stabilization of the compound. Diethyl ether or Tetrahydrofuran (THF) are the two commonly used ethereal solvents. Diethyl ether is used over tetrahydrofuran due to cost and the ability to be easily removed from the solution (1). Use caution when opening diethyl ether and tetrahydrofuran containers because they have the ability to create hydroperoxides, which are dangerous because they are explosives
research,forensics,environmental testing, and many more fields because it is simple and inexpensive way to analyze small samples. In this experiment two compounds (solid) were used ferrocene and acetylferrocene. In the first step 50 ml of 2:8 diethyl ether/petroleum ether was placed in an erlenmeyer flask covered with a parafilm paper to avoid evaporation. Then the glass column was prepared placing a small cotton on the bottom of the glass column and then added a small amount of sand , wich will give the
create good carboxylate electrophiles, as elucidated by Li, et al.2 Figure 1: Preparation of Grignard Reagent (Phenylmagnesium Bromide) In this experiment, a Grignard reagent was prepared using bromobenzene and magnesium in diethyl ether (Figure 1). An aprotic solvent (diethyl ether) was used because Mg0 reacts readily with protic solvents to form Mg2+. Figure 2: Formation of 1,1-Diphenylethanol with Grignard Reagent Afterwards, the Grignard reagent was added to acetophenone to form 1,1-diphenylethanol
layers were also formed: the upper ether layer with the product, triphenylmethanol, and the lower aqueous layer that contained the hydrochloric acid and inorganic compounds. Since neutralization involves heat, some ether was lost to evaporation and additional ether was added to maintain a sufficient volume in the upper organic layer. (Pavia et al 278). The lower layer was then extracted by a separatory funnel. The layer was extracted, and then reextracted with ether, as quickly as possibly, because
Palha s3333523 Experiment 2: Williamson Ether Synthesis of 2-octadecyloxynaphthalene Demonstrator: P. Kabauri Date of experiment: 26-09-2017 Summary: In this experiment, 2-octadecylooxnapthalene was synthesized. The synthesis consists of making 2-naphthol solution with acetonitrile. Then CsCO3 and bromooctadecane was added to the solution. And at the end we crystalized it and found out the melting point which ranged from 64-68°C. Theory: In order for an ether to be produced we needed an aroxide ion
Filtration – This is an experiment whereby inorganic and displacement chemical reactions take place to collect a salt and produce water through the process of filtration. The chemicals used were a metal oxide, in this case, copper oxide and a dilute acid, sulphuric acid, aiming to separate the copper and oxygen to collect the pure copper (II) ions, which is a soluble salt. The colour should be a very characteristic blue. Sulfuric acid is added to a beaker. A tripod and Bunsen burner is set up and