Lab Report Calorimetry

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Introduction The objective of the experiment is to utilize a calorimeter to observe the changes of thermodynamic quantities. For Part 1: Heat of a Neutralization Reaction, 50.0 mL of 2.0 M NaOH was added and mixed with 50.0 mL of 2.0 M HCl in a calorimeter to in order to calculate the heat of neutralization for a strong acid/strong base reaction. For Part 2: Specific Heat Capacity of a Metal, an unknown metal (either A, B, or E), was heated in boiling water, and the unknown metal was placed and mixed in a calorimeter with cold tap water, and the unknown metal was identified. For Part 3: Molar Heat of Solution of a Salt, ammonium chloride salt (NH4Cl) was added and mixed in a calorimeter with deionized water, and the molar heat of solution …show more content…

The materials used during Part 2 of the experiment includes an unknown metal (either A, B, or E), an analytical balance 200 mL of tap water, a 400 mL beaker, a hot plate, 50.0 mL of cold water, and a calorimeter. The materials used during Part 3 of the experiment includes 50.0 mL of deionized water, 2 g of NH4Cl, an analytical balance and a …show more content…

Graph of Temperature (°C) vs. Time (seconds) of NH4Cl solution in a calorimeter with deionized water.

Discussion, Conclusion, and Focus Questions
The heat of neutralization for a strong acid/ strong base reaction such as 50.0 mL of 2.0 M NaOH neutralized with 50.0 mL of 2.0 M HCl is -33.86 kJ/mol, and is an exothermic reaction.
The identity of the unknown metal, e, was found to be copper because the specific heat capacity of the unknown metal, e, was 0.314 J/g°C, and according to “Table: Specific Heat Capacities of Some Substances” (Smeureanu & Geggier, 2016, p. 132) was closest to the value of 0.385, in which the substance is copper.
The molar heat of solution of ammonium chloride salt was found to be 9.6 kJ/mol and is an endothermic reaction. Because the literature value of NH4Cl is 14.78 kJ/mol, there may be various possible experimental errors in which the NH4Cl, was not dissolved and mixed thoroughly in the water, insulation errors of the calorimeter, faulty thermometers resulting in inaccurate readings, and measurement errors.
References
Smeureanu, G., and Geggier, S. “General Chemistry Laboratory”, Hunter College. N.Y. 2015, pp.129 - 134.
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