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Acetylsalicylic acid lab report
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Lab Report The Preparation of Organic Compounds Aspirins and Oil of Wintergreen Introduction The purpose of this experiment is to prepare two organic compounds (aspirin and oil of wintergreen) and to illustrate the typical organic reactions. Students will also learn some techniques commonly used in organic synthesis and the meaning of the terms theoretical yield, actual yield, and percent yield. Both Aspirin (acetylsalicylic acid) and oil of wintergreen (methyl salicylate) are commonly used organic compounds. Aspirin is usually used as a pain reliever or fever reducer, and oil of wintergreen is used in rubbing liniments for sore muscles and as a flavoring agent. Aspirin is usually made by reacting salicylic acid with acetic anhydride. C7H6O3 + C4H6O3 C9H8O4 + C2H4O2 (salicylic acid) (acetic anhydride) (acetyl salicylic acid: aspirin) (acetic acid) Oil of wintergreen is made by reacting salicylic acid with methanol in the presence of sulfuric acid. C7H6O3 + CH4O C8H8O4 + H2O (salicylic acid) (methanol) (methyl salicylate: oil of wintergreen) (water) Procedure Preparation of Aspirin 1. Set up a water bath and an ice bath. 2. Put 3 grams of salicylic acid and 4mL of acetic anhydride in 125mL conical flask. 3. While swirling the flask, add 5 drops of concentrated sulfuric acid to the mixture. 4. Heat the flask in the beaker of boiling water for 15 minutes or until the solid dissolves. 5. Carefully remove the flask with 9" tongs from the water bath and add 25mL of your ice-cold water to the flask. 6. Set the flask in the ice bath until crystallization appears to be complete.
Each subsequent trial will use one gram more. 2.Put baking soda into reaction vessel. 3.Measure 40 mL vinegar. 4.Completely fill 1000 mL graduated cylinder with water.
2. Drop a gummy bear into each of your prepared beaker or cup and place the beaker or cup
the large beaker pour in some more hot water or if it is too hot pour
4. Pour about 300mL of tap water into the beaker. Set up a hot-water bath using a hot plate, retort stand, and thermometer clamp. Alternatively, use a Bunsen burner, retort stand, ring clamp, thermometer clamp, and wire gauze.
Then the flask needs to be filled with 20 cm3 Hcl acid, the acid is
x cm's of elodia and put it in the beaker. Cover the elodia with the
Plan 1. Collect 4 different sized beakers 2. Boil some water in the kettle 3. Pour 50ml into each beaker 4. After 1 minute check temperature 5.
Rinse your beaker thoroughly to wash any excess powder. 12. Repeat steps 7-11 3 more times for reliability. To make sure the temperature still stays hot by continue heating the water a little bit using the hot plate. 13.
7.) After you have heated them to the right temperatures, pour the excess water into a dry evaporating dish. ( Be sure not to get any of the substance in your solution. )
put it in a conical flask. I will put the flask on top of a piece of
Background Information Aspirin is an analgesic (pain relieving) and an antipyretic drug (a drug that lowers body temperature). The main constituent of aspirin is 2 - ethanoythydroxybenzoic acid, also known as acetylsalicyclic acid (shown below right). It was originally made from just salicylic acid (which is found in the bark of a willow tree) when used by the Ancient Greeks to counter fever and pain, but its bitterness and tendency to irritate the stomach caused problems. These were resolved by the German chemist Felix Hoffman, who made the acetyl derivative of salicylic acid in the
2. In the large beaker, put water and boil it completely. After that, remove the beaker from heat. 3. Sample tubes (A-D) should be labeled and capped tightly.
We decided to use 2 minutes, as this gave the best results. We repeated the experiment fifteen times, firstly heating 50cm3 three. times, then add 25cm3 of water each time, so from 50cm3 to 350cm3. After each repetition we rinsed the beaker so as to make this a fair. experiment.
needed are a small bowl of warm water in which there is a squirt of
tube. Add 6 mL of 0.1M HCl to the first test tube, then 0.1M KMnO4 and