Finding out How Much Acid There is in a Solution

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Finding out How Much Acid There is in a Solution

During the extraction of a metal from its ore, sulphur dioxide is

often produced. It is converted into Sulphuric (VI) acid and sold as a

useful by-product.

I shall be carrying out a titration between sodium carbonate, a weak

alkali, and sulphuric acid, a strong acid, to calculate the

concentration of the sulphuric acid. The sodium carbonate sample I

shall be using is a solid. Solids cannot be titrated successfully, so

I will turn it into a solution by adding distilled water to it. The

distilled water has no adverse effects on the sodium carbonate.

[IMAGE]Na2CO3(aq) + H2SO4(aq) Na2SO4(aq) + H2O(l) + CO2(g)

Methyl orange is an acid-base indicator, which changes colour

according to the hydrogen ion concentration of the solution to which

it is added to. It 'indicates' the end point of the acid-base

titration, and tests the acidity or alkalinity of the solution. I

shall be using methyl orange as the indicator in my titration because,

for a titration between a strong acid and a weak alkali, methyl orange

works most effectively.

HMe H + Me

Red colourless Yellow

From this titration, I can expect the solution to turn colourless.

This is because the addition of an acid displaces the equilibrium to

the left so that the concentration of H is more than Me and so the

solution turns clear.

Apparatus

Ø Sample of sodium carbonate (2.63g)

Ø Sulphuric acid

Ø Methyl orange indicator (3 drops)

Ø Distilled water

Ø Spatula

Ø Watch Glass (23.56g)

Ø Glass rod

Ø 250cm³ Beaker x2

Ø 250cm³ Volumetric flask

Ø 250cm³ Conical flask

Ø Funnel

Ø 25cm³ Pipette and pipette filler

Ø Burette

Ø Weighing scales

Ø White tile

Ø Safety glasses/lab coat

Ø Dropping pipette

N.B All the apparatus above is accurately calibrated.

Variables

The control variables, which are the factors I shall be keeping the

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